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The First Application of Palladium–Phosphorus Catalysts in the Direct Synthesis of Hydrogen Peroxide: Reasons for the Promoting Action of Phosphorus Научная публикация

Журнал Kinetics and Catalysis
ISSN: 0023-1584 , E-ISSN: 1608-3210
Вых. Данные Год: 2023, Том: 64, Номер: 6, Страницы: 804–814 Страниц : DOI: 10.1134/S0023158423060022
Авторы Belykh L.B. 1 , Skripov N.I. 1 , Sterenchuk T.P. 1 , Akimov V.V. 2 , Tauson V.L. 2 , Likhatski M.N. 3 , Milenkaya E.A. 1 , Kornaukhova T.A. 1 , Schmidt F.K. 1
Организации
1 Irkutsk State University, Irkutsk, 664003 Russia
2 Vinogradov Institute of Geochemistry, Siberian Branch, Russian Academy of Sciences, Irkutsk, 664033 Russia
3 Institute of Chemistry and Chemical Technology, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk, 660036 Russia
Реферат: The main reasons for the promoting effect of phosphorus on the properties of Pd–P/ZSM-5 catalysts during direct synthesis of H2O2 from H2 and O2 under mild conditions are considered based on the data obtained by X-ray photoelectron spectroscopy (XPS), X-ray powder diffraction (XRD), high-resolution transmission electron microscopy (HRTEM), and inductively coupled plasma mass spectrometry (ICP MS). The introduction of phosphorus in the catalyst affects the particle size and the electronic state of palladium in the surface layer, as well as the surface concentration of the phosphate and phosphite ions. The yield of H2O2 increases when the particle size of the Pd–P catalysts decreases, when the side process of H2O2 decomposition is inhibited by the phosphate and phosphite surface ions, and when the hydrogen solubility in the solid solutions of phosphorus in palladium decreases.
Библиографическая ссылка: Belykh L.B. , Skripov N.I. , Sterenchuk T.P. , Akimov V.V. , Tauson V.L. , Likhatski M.N. , Milenkaya E.A. , Kornaukhova T.A. , Schmidt F.K.
The First Application of Palladium–Phosphorus Catalysts in the Direct Synthesis of Hydrogen Peroxide: Reasons for the Promoting Action of Phosphorus
Kinetics and Catalysis. 2023. V.64. N6. P.804–814. DOI: 10.1134/S0023158423060022 WOS Scopus РИНЦ CAPlusCA OpenAlex
Оригинальная версия: Белых Л.Б. , Скрипов Н.И. , Стеренчук Т.П. , Акимов В.В. , Таусон В.Л. , Лихацкий М.Н. , Миленькая Е.А. , Корнаухова Т.А. , Шмидт Ф.К.
Первое применение палладий-фосфорных катализаторов в прямом синтезе пероксида водорода: причины промотирующего действия фосфора
Кинетика и катализ. 2023. Т.64. №6. С.749-760. DOI: 10.31857/S0453881123060023 РИНЦ OpenAlex
Даты:
Поступила в редакцию: 21 мар. 2023 г.
Принята к публикации: 16 мая 2023 г.
Опубликована online: 12 дек. 2023 г.
Идентификаторы БД:
Web of science: WOS:001122621800007
Scopus: 2-s2.0-85179677594
РИНЦ: 64671262
Chemical Abstracts: 2023:2603181
Chemical Abstracts (print): 185:200452
OpenAlex: W4389615944
Цитирование в БД:
БД Цитирований
Scopus 3
Web of science 1
OpenAlex 3
Альметрики: