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Experimental and Theoretical Studies of the Electronic Spectra of Mixed Framework Phosphates of Zr and Co Научная публикация

Журнал The Journal of Physical Chemistry B
ISSN: 1520-6106 , E-ISSN: 1520-5207
Вых. Данные Год: 2004, Том: 108, Номер: 22, Страницы: 6969-6980 Страниц : 12 DOI: 10.1021/jp0363500
Авторы Frolova Yulia V. 1,2 , Avdeev Vasilii I. 2 , Ruzankin Sergey Ph. 2 , Zhidomirov Georgii M. 2 , Fedotov Martin A. 2 , Sadykov Vladislav A. 1,2
Организации
1 Novosibirsk State University
2 Boreskov Institute of Catalysis, Novosibirsk 630090, Russia
Реферат: Electronic diffuse reflectance spectra were acquired for samples of mixed framework phosphates of zirconium and cobalt calcined in a broad temperature range (40−900 °C). Analysis of the spectral features and their comparison with data available for different cobalt phosphates and CoAPO revealed that in complex framework phosphates the nearest coordination sphere of Co cations corresponds mainly to the oxygen polyhedra with a low coordination number such as the tetrahedron, pyramid, etc. In the frames of the time-dependent DFT method (TDDFT), the electronic excitation energies for cobalt cations in different oxygen environments have been calculated. The results obtained allowed us to describe the spectra of mixed cobalt−zirconium phosphates of various crystallinity both in the d−d transition and charge-transfer ranges with due regard for the simultaneous presence of Co cations in different coordination polyhedra and spin states. In prediction of the spectral features, the approach used in this work was shown to reasonably agree with the traditional concepts and experience in analysis of the electronic spectra of transition metal cations in their complexes and inorganic frameworks.
Библиографическая ссылка: Frolova Y.V. , Avdeev V.I. , Ruzankin S.P. , Zhidomirov G.M. , Fedotov M.A. , Sadykov V.A.
Experimental and Theoretical Studies of the Electronic Spectra of Mixed Framework Phosphates of Zr and Co
The Journal of Physical Chemistry B. 2004. V.108. N22. P.6969-6980. DOI: 10.1021/jp0363500 WOS Scopus РИНЦ CAPlusCA OpenAlex Sciact
Даты:
Поступила в редакцию: 8 авг. 2003 г.
Принята к публикации: 25 мар. 2004 г.
Опубликована online: 7 мая 2004 г.
Опубликована в печати: 1 июн. 2004 г.
Идентификаторы БД:
Web of science: WOS:000221700300015
Scopus: 2-s2.0-2942726430
РИНЦ: 13452227
Chemical Abstracts: 2004:369137
Chemical Abstracts (print): 141:95943
OpenAlex: W2049269701
Sciact: 9989
Цитирование в БД:
БД Цитирований
Scopus 4
OpenAlex 3
Альметрики: