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Ex Situ EPR Investigation of MoO3/Al2O3 Catalysts for Propylene Metathesis Научная публикация

Конференция VI Всероссийская научно молодежная школа-конференция "Химия под знаком СИГМА: исследования, инновации, технологии"
18-20 мая 2020 , Омск
Журнал AIP Conference Proceedings
ISSN: 0094-243X , E-ISSN: 1551-7616
Вых. Данные Год: 2020, Том: 2301, Номер статьи : 040020, Страниц : 4 DOI: 10.1063/5.0032830
Авторы Yurpalov V.L. 1 , Karpova T.R. 1 , Moiseenko M.A. 1 , Drozdov V.A. 1 , Buluchevskiy E.A. 1 , Lavrenov A.V. 1
Организации
1 Center of New Chemical Technologies BIC, Boreskov Institute of Catalysis, 54, Neftezavodskaya Str., Omsk 644040, Russian Federation
Реферат: A series of propylene metathesis MoO3/Al2O3 catalysts (2–10 wt. % of MoO3) activated in Ar and under ex situ reaction conditions was studied by EPR spectroscopy. Similar EPR signals from surface molybdate clusters (Mo5+) were observed for each sample. The concentration of pentavalent molybdenum in paramagnetic form determined by EPR increases with an increase in the MoO3 content from 2 to 5 wt. %, then changes slightly. It was also found that the activity of the catalysts in the propylene metathesis reaction is proportional to the increment in the concentration of Mo5+ paramagnetic species determined after contact with propylene. This indicates that higher oxidation states of molybdenum form active paramagnetic complexes during the reaction with propylene.
Библиографическая ссылка: Yurpalov V.L. , Karpova T.R. , Moiseenko M.A. , Drozdov V.A. , Buluchevskiy E.A. , Lavrenov A.V.
Ex Situ EPR Investigation of MoO3/Al2O3 Catalysts for Propylene Metathesis
AIP Conference Proceedings. 2020. V.2301. 040020 :1-4. DOI: 10.1063/5.0032830 Scopus РИНЦ CAPlusCA OpenAlex Sciact publication_identifier_short.sciact_ihcp_identifier_type
Даты:
Опубликована online: 8 дек. 2020 г.
Идентификаторы БД:
Scopus: 2-s2.0-85098087728
РИНЦ: 45058107
Chemical Abstracts: 2021:1128914
Chemical Abstracts (print): 175:131803
OpenAlex: W3112775972
Sciact: 49879
publication_identifier.sciact_ihcp_identifier_type: 3293
Цитирование в БД:
БД Цитирований
Scopus 2
OpenAlex 1
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